| 1985 |
The PH-20 surface antigen on guinea pig sperm posterior head plasma membrane has a required function in sperm binding to the egg zona pellucida; monoclonal antibody PH-20 MAb inhibited sperm-zona binding ~90%, establishing PH-20 as essential for zona adhesion. |
Monoclonal antibody inhibition of sperm-zona binding assay; competitive binding with 125I-labeled MAbs |
The Journal of cell biology |
High |
4066757
|
| 1986 |
After the acrosome reaction (exocytosis), the intracellular PH-20 population on the inner acrosomal membrane (IAM) is inserted into the plasma membrane, producing an ~3-fold increase in surface PH-20 antigen; this reveals a mechanism for rapid upregulation of a sperm surface protein via exocytosis. |
Indirect immunofluorescence; quantification of antigenic sites before and after acrosome reaction; permeabilization of acrosome-intact sperm |
The Journal of cell biology |
High |
3771636
|
| 1987 |
PH-20 protein reaches the sperm plasma membrane via two transport pathways during spermiogenesis: first inserted into the acrosomal membrane, then separately into the plasma membrane; both populations are initially uniformly distributed and later become restricted to specific domains, indicating localization occurs post-insertion rather than by intracellular sorting. |
Developmental immunofluorescence localization during spermiogenesis; SDS-PAGE of testicular cell extracts |
Developmental biology |
Medium |
3305112
|
| 1987 |
PH-20 on the posterior head plasma membrane of acrosome-intact sperm is mobile (D = 1.8×10⁻¹⁰ cm²/s) but restricted ~50-fold relative to lipid; after migration to the IAM of acrosome-reacted sperm it diffuses freely (D = 4.9×10⁻⁹ cm²/s, similar to lipid), supporting a barrier-to-diffusion model for domain maintenance. |
Fluorescence redistribution after photobleaching (FRAP) on individual sperm |
The Journal of cell biology |
High |
3558486
|
| 1988 |
PH-20 is anchored in the sperm plasma membrane via a glycosylphosphatidylinositol (GPI/phosphatidylinositol lipid) anchor, and its lateral diffusion rate is >1000-fold slower than lipid diffusion, indicating that ectodomain interactions constrain mobility of a GPI-anchored protein. |
Phosphatidylinositol-specific phospholipase C (PI-PLC) cleavage; FRAP measurement of diffusion rates |
Science |
High |
3381102
|
| 1988 |
PH-20 purified from guinea pig sperm by monoclonal antibody affinity chromatography exists in three forms: 64 kDa, 56 kDa, and an endoproteolytically cleaved form of two disulfide-linked fragments (~41–48 kDa and ~27 kDa), indicating site-specific endoproteolysis occurs in sperm preparations. |
Monoclonal antibody affinity purification; SDS-PAGE; Cleveland digest analysis |
Biology of reproduction |
Medium |
3042032
|
| 1990 |
cDNA cloning of guinea pig PH-20 revealed a novel protein of 468 amino acids with six N-linked glycosylation sites, twelve cysteines (eight clustered near the C-terminus), encoded by a single gene with a single ~2.2 kb mRNA; Southern blots confirmed a single gene and conservation across multiple mammalian species. |
cDNA cloning, sequencing; Southern blot; Northern blot |
The Journal of cell biology |
High |
2269661
|
| 1991 |
PH-20 protein migration from the posterior head plasma membrane to the inner acrosomal membrane after the acrosome reaction occurs against a concentration gradient and is calcium-dependent, arguing against passive diffusion–trapping and in favor of an active translocation mechanism. |
Fluorescence microscopy with digital image processing of individual sperm; calcium manipulation |
Developmental biology |
Medium |
1995397
|
| 1993 |
Human PH-20 protein expressed in RK13 cells using a vaccinia virus system has hyaluronidase activity; PI-PLC treatment releases the enzyme from the cell surface with a large increase in activity, confirming the GPI anchor and hyaluronidase function of human PH-20. |
Vaccinia virus expression; hyaluronidase activity assay; PI-PLC release |
FEBS letters |
High |
8282124
|
| 1993 |
Human and cynomolgus monkey PH-20 cDNAs were isolated; human PH-20 encodes 509 residues, is 59% identical to guinea pig PH-20, and its mRNA is strictly testis-specific (single 2.4 kb transcript) with a single gene in the human genome. |
cDNA cloning; Southern blot; Northern blot of 16 human tissues |
Proceedings of the National Academy of Sciences of the United States of America |
High |
8234258
|
| 1994 |
Sperm plasma membrane protein PH-20 has hyaluronidase activity enabling acrosome-intact sperm to penetrate the cumulus cell layer; purified recombinant PH-20 disperses cumulus cells from mouse eggs, and anti-PH-20 antibodies prevent acrosome-intact sperm from passing through the cumulus to reach the zona pellucida. |
In vitro cumulus penetration assay; treatment with purified recombinant PH-20; antibody-blocking experiments |
The Journal of cell biology |
High |
8195297
|
| 1995 |
Human SPAM1 gene maps to chromosome 7q31, is encoded by at least 4 exons spanning ~11 kb of genomic DNA, and expression as a 2.4 kb transcript is strictly limited to testis in a panel of 16 human tissues. |
FISH; somatic cell hybrid PCR; Northern blot; genomic Southern blot |
Genomics |
High |
8575780
|
| 1996 |
PH-20 is bifunctional: it has a hyaluronidase activity required for cumulus penetration and a separate, distinct activity required for secondary sperm-zona binding. Anti-PH-20 MAb that blocks zona binding (90%) has no effect on hyaluronidase activity; apigenin blocks hyaluronidase 93% without inhibiting zona binding; pretreatment of oocytes with hyaluronidase to remove zona HA does not affect secondary zona binding. |
Antibody inhibition assays; apigenin (hyaluronidase inhibitor) assays; zona pretreatment with hyaluronidase; sperm-zona binding assays |
Biology of reproduction |
High |
8793062
|
| 1996 |
The soluble hyaluronidase released from guinea pig sperm at the acrosome reaction is a soluble form of PH-20 (sPH-20): anti-PH-20 antiserum recognizes it by immunoblot, completely inhibits its enzymatic activity, and 97% is removed by anti-PH-20 affinity chromatography; sPH-20 is not endoproteolytically cleaved unlike membrane PH-20, suggesting enzymatic release from its GPI anchor. |
Immunoblot; immunoaffinity chromatography; enzyme activity inhibition; anti-PH-20 antiserum |
Biology of reproduction |
High |
8724363
|
| 1996 |
Cynomolgus macaque sperm PH-20 exists as a 64 kDa form on the plasma and inner acrosomal membranes and a 53 kDa form released during acrosome reaction; the 64 kDa form has predominantly neutral pH hyaluronidase activity while the 53 kDa form has acid-active hyaluronidase activity; apigenin inhibits both. |
Western blot; HA substrate gel electrophoresis; ELISA hyaluronidase assay; Fab-immunolocalization; ultrastructure |
Developmental biology |
High |
8608861
|
| 1997 |
The soluble 60 kDa hyaluronidase from bovine testes is a fragment of the membrane-bound PH-20 enzyme; peptide sequencing of 44 fragments from the purified 60 kDa protein aligned to the PH-20 cDNA sequence; it lacks the signal peptide and 56 C-terminal amino acids including the GPI-anchor site. |
cDNA cloning; protein purification; protease/cyanogen bromide digestion with peptide sequencing |
FEBS letters |
High |
9280317
|
| 1997 |
PH-20 N-terminal domain contains the hyaluronidase activity (based on homology with bee venom hyaluronidase and functional data); it is GPI-anchored; its dual roles in cumulus penetration (plasma membrane form, neutral pH activity) and secondary zona binding (inner acrosomal membrane form, post-acrosome reaction) are biochemically distinct. |
Synthesis of review of functional data; domain analysis from cDNA sequence; functional assays cited |
Biology of reproduction |
Medium |
9116127
|
| 1997 |
In male guinea pigs immunized with PH-20, infertility is associated with emptying of the cauda epididymis (no normal sperm) and induction of experimental autoimmune orchitis (EAO); this is the first demonstration that a purified sperm molecule of known function can induce EAO. |
Immunization; histopathology; antibody titer measurement; immunofluorescence of germ cells |
Biology of reproduction |
Medium |
9160711
|
| 1998 |
Hyaluronic acid (HA) interacts with PH-20 on human sperm to increase basal intracellular calcium and potentiate the acrosome reaction induced by progesterone or zona pellucida; blocking PH-20 with anti-PH-20 Fab abolished the HA-mediated Ca²⁺ increase and enhancement of acrosome reactions. |
Acrosome reaction assay; intracellular calcium measurement; Fab fragment blocking of PH-20 |
Zygote |
High |
9770775
|
| 1999 |
Murine Spam1 (PH-20) gene promoter contains a CRE (cAMP-responsive element) at position -57 that binds CREM in testicular nuclear extracts; in vitro transcription assays show CRE is necessary for promoter activity; Spam1 transcripts are absent in CREM-knockout mice, establishing CREM as a transcriptional regulator of Spam1. |
Gel mobility shift assay; in vitro transcription; Northern blot of CREM-KO mice; primer extension |
Molecular reproduction and development |
High |
10423292
|
| 1999 |
Biochemical maturation of Spam1 during epididymal transit involves N-linked oligosaccharide modification: caput sperm have a larger ~74 kDa form with lower hyaluronidase activity, while caudal sperm have a ~67 kDa form with 4.3-fold higher activity; enzymatic deglycosylation of both reduces to ~56 kDa backbone, and all four N-glycosylation sites are functional. |
Immunofluorescence; Western blot; enzymatic deglycosylation; hyaluronidase activity assay |
Molecular reproduction and development |
High |
9890751
|
| 1999 |
HA increases intracellular Ca²⁺ in macaque sperm through plasma membrane PH-20; anti-PH-20 Fab fragments inhibit the Ca²⁺ increase induced by HA, HA gels, and cumulus masses; FITC-HA binding to sperm is localized over the acrosome (PH-20 location) and is inhibited by anti-PH-20 Fab. PH-20 aggregation (by bivalent antibody or zona pellucida binding) is associated with increased Ca²⁺ and acrosome reaction. |
Fluorometry with Fluo-3 Ca²⁺ indicator; Fab fragment blocking; FITC-HA binding; video imaging; TEM |
Zygote |
High |
10533704
|
| 1999 |
PH-20 (but not acrosin) is required for secondary sperm-zona binding and zona penetration in macaque; anti-PH-20 IgG completely blocked zona penetration while anti-acrosin and anti-CD46 IgG had no effect; PH-20 is present on the inner acrosomal membrane of zona-bound acrosome-reacted sperm whereas acrosin is not. |
Immunolocalization by TEM; sperm-zona penetration assay with blocking antibodies (up to 300 µg/ml) |
Molecular reproduction and development |
High |
10369396
|
| 2001 |
A region of macaque PH-20 (Peptide 2, aa 205-235) functions as a HA-binding domain separate from the catalytic hyaluronidase domain; recombinant PH-20 protein lacking this region (E12) does not bind HA, while the full N-terminal construct (G3) binds biotinylated HA; anti-Peptide 2 Fab inhibits HA-induced Ca²⁺ increase in sperm, linking this domain to cell signaling. |
Recombinant protein binding assay; photoaffinity HA crosslinking; microplate HA binding assay; Fab inhibition of intracellular Ca²⁺ |
Molecular reproduction and development |
High |
11746965
|
| 2001 |
PH-20 plasma membrane form mediates HA-induced intracellular signaling via a HA-binding domain distinct from hyaluronidase domains; signaling involves Ca²⁺ increase and aggregation of GPI-anchored PH-20 in the plasma membrane; a 92-kDa protein may be the cytoplasmic signaling molecule linked to PH-20. |
Review and synthesis of functional data; signaling assays; antibody-induced PH-20 aggregation; calcium measurements |
Matrix biology |
Medium |
11731269
|
| 2001 |
Despite absence of PH-20 in Spam1 null mice produced by homologous recombination, male mice are fertile; PH-20-null sperm show reduced cumulus dispersal (delayed fertilization at early time points only) but retain fertilizing ability due to other hyaluronidases present in the acrosome detected by Western blot. |
Homologous recombination knockout; in vitro fertilization assay; Western blot for other hyaluronidases |
The Journal of biological chemistry |
High |
12065596
|
| 2001 |
Spam1 is haploid expressed in mouse spermatids with both mRNA and protein compartmentalized (non-shared) among conjoined spermatids; this lack of transcript sharing via intercellular bridges leads to biochemically different sperm populations, providing a mechanism for transmission ratio distortion (TRD) in heterozygous males. |
RNA FISH; immunocytochemistry; flow cytometry; confocal microscopy; temporal expression analysis |
Biology of reproduction |
High |
11369602
|
| 2002 |
Hyaluronidase activity of macaque sperm surface PH-20 requires both N-linked glycosylation (removal abolishes activity) and disulfide bond integrity (reduction with β-mercaptoethanol or DTT abolishes activity); mannose is a major sugar in the N-linked glycans; 6 isoforms with pI 5.1–6.0 were identified by 2D electrophoresis. |
Immunoaffinity purification; N-glycosidase F deglycosylation; β-mercaptoethanol/DTT reduction; lectin blotting; 2D electrophoresis; hyaluronidase activity assay |
Journal of andrology |
High |
11868814
|
| 2003 |
Mouse Spam1 is transcribed in the female genital tract (uterus, oviduct, vagina) in a region-dependent manner; the protein has hyaluronidase activity at neutral pH but not acidic pH in female tissues, and its expression in the uterus fluctuates with the estrous cycle. |
RT-PCR; RNase protection assay; in situ transcript hybridization; Western blot; immunohistochemistry; HA substrate gel electrophoresis |
Biology of reproduction |
Medium |
12672666
|
| 2003 |
Epididymal SPAM1 is released with its intact GPI lipid anchor predominantly in insoluble particles in luminal fluid; PI-PLC treatment or Triton X-100 releases the majority, confirming lipid anchor retention on secreted protein; two-dimensional gel shows distinct isoforms in epididymis vs. testis, with N-linked and O-linked glycosylation differences. |
Ultracentrifugation; PI-PLC treatment; 2D-PAGE with immunoblotting; lectin blotting; enzymatic deglycosylation |
Journal of andrology |
High |
12514083
|
| 2004 |
Spam1 mRNA in mouse spermatids is localized near the ER and anchored to the cytoskeleton, absent from intercellular bridges; this compartmentalization mediates non-sharing of transcripts. Spam1 on caudal sperm surface mediates the synergistic increase in acrosome reactions induced by HA and progesterone, confirmed by reduced response in Rb(6.16) Spam1 mutant sperm. |
In situ hybridization by light and electron microscopy; immunocytochemistry; acrosome reaction assay with HA+progesterone; comparison to Spam1 mutant mice |
Molecular reproduction and development |
Medium |
15457544
|
| 2005 |
HYAL5 (a GPI-anchored hyaluronidase active at pH 5–7) is expressed exclusively in testis and is present on sperm plasma and acrosomal membranes; it can disperse cumulus cells and is the principal cumulus matrix depolymerase in mouse sperm when PH-20 is absent, while PH-20 compensates for Hyal5's role. |
Protein purification from PH-20-null sperm; hyaluronan zymography; cumulus dispersal assay; apigenin inhibition; GPI-anchor characterization |
Proceedings of the National Academy of Sciences of the United States of America |
High |
16330764
|
| 2005 |
Spam1 mRNA 3'UTR AU-rich elements (AREs) bind six testicular cytoplasmic proteins (AU-binding proteins, AUBPs) that interact with the cytoskeleton; these interactions mediate post-transcriptional regulation of Spam1 in spermatids; antisense RNA in testis can modulate ARE function. Transgenic overexpression attempts failed, indicating tight post-transcriptional control. |
UV cross-linking assay; transgenic overexpression; Northern analysis; cytoskeletal binding experiments |
Molecular reproduction and development |
Medium |
16250006
|
| 2005 |
Spam1 RNA is anchored to the cytoskeleton in spermatids and interacts via 3' UTR AU-rich sequences with cytoskeletal-associated AU-binding proteins, preventing transcript sharing through intercellular bridges; this mechanism drives TRD. Spam1 overexpression (transgene) causes TRD by producing sperm with cytoplasmic droplets containing excess Spam1, reducing fertilizing ability. |
EM in situ hybridization; Northern analysis of fractionated testicular RNA; UV cross-linking; flow cytometry; FISH |
Reproductive biology and endocrinology |
High |
16092963
|
| 2006 |
Epididymal SPAM1 acquired by Spam1-null sperm from wild-type epididymal luminal fluid in vitro significantly increases cumulus penetration ability, directly linking epididymal SPAM1 uptake with fertilizing ability and establishing it as a marker of sperm maturation. |
In vitro incubation of null sperm with WT epididymal luminal fluid; flow cytometry; immunocytochemistry; IVF cumulus penetration assay |
Biology of reproduction |
High |
16436526
|
| 2007 |
Recombinant mouse SPAM1 and HYAL5 expressed in Xenopus oocytes both exhibit hyaluronidase activity at neutral pH and are GPI-anchored; HYALP1 lacks hyaluronidase activity despite sequence similarity. |
Recombinant expression in Xenopus oocytes; hyaluronidase activity assay; GPI-anchor characterization |
The Biochemical journal |
High |
16925524
|
| 2007 |
Human recombinant PH-20 expressed in Drosophila S2 cells uses an HA octasaccharide as its minimum substrate (not hexasaccharide as for bovine testicular hyaluronidase); PH-20 catalyzes both hydrolysis and transglycosylation of HA octasaccharide. |
Recombinant expression; capillary zone electrophoresis analysis of reaction products; minimum substrate determination |
Glycobiology |
High |
17602139
|
| 2008 |
SPAM1 is transferred to sperm from murine epididymosomes (male) and newly identified uterosomes (female) via a vesicular docking mechanism; uptake requires the intact GPI anchor (abolished by enzymatic anchor cleavage); fluorescently labeled vesicles are observed juxtaposed to sperm plasma membranes by TEM. |
Ultracentrifugation; immunogold labeling; confocal and TEM microscopy; GPI anchor cleavage experiments; fluorescent vesicle tracking |
Molecular reproduction and development |
High |
18384048
|
| 2009 |
SPAM1 is required for efficient sperm entry into and penetration through the cumulus matrix; SPAM1-null sperm accumulate at the surface/outer edge of the cumulus, while HYAL5-null sperm show no such defect; double comparison demonstrates SPAM1 but not HYAL5 is the functionally critical hyaluronidase for cumulus entry. |
HYAL5 knockout mouse generation; in vitro fertilization assay; comparative analysis of WT, HYAL5-null, and SPAM1-null sperm |
Biology of reproduction |
High |
19605784
|
| 2009 |
Clusterin (CLU) in epididymal/uterine luminal fluid stabilizes monomeric GPI-linked SPAM1 and mediates its transfer to human and mouse sperm membranes; anti-CLU antibody reduces SPAM1 delivery; co-immunoprecipitation reveals direct CLU-SPAM1 association; high CLU concentrations reduce and low concentrations enhance SPAM1 transfer. |
Co-immunoprecipitation; native Western blot; anti-CLU antibody blocking; dose-response transfer assay; apolipoprotein-enhanced transfer |
Biology of reproduction |
High |
19357365
|
| 2024 |
Cryo-EM structure of human PH-20 shows: a central catalytic domain with conserved catalytically essential residues; a unique EGF-like domain with a longer sequence forming a flexibly anchored β-hairpin containing a disulfide bond, distinguishing it from other hyaluronidase family members. |
Cryogenic electron microscopy (cryo-EM); structural comparison with other hyaluronidase structures |
Proteins |
High |
39722545
|